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Read e-book online Advances in Atomic Spectroscopy, Volume 3 (Advances in PDF

By J. Sneddon

This sequence describes chosen advances within the sector of atomic spectroscopy. it's essentially meant for the reader who has a heritage in atmoic spectroscopy; appropriate to the amateur and professional. even though a frequent and authorised process for steel and non-metal research in quite a few complicated samples, Advances in Atomic Spectroscopy covers quite a lot of fabrics. each one bankruptcy will thoroughly conceal a space of atomic spectroscopy the place quick improvement has happened.

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1990). g. reducing the selenium and arsenic species to Se TM and As Iu, respectively, using a reagent such as hydrochloric acid or L-cysteine. g. arsenobetaine and selenomethionine, which are extremely stable. To destroy these compounds, either very harsh acidic conditions such as perchloric acid are required, which can on occasions be hazardous for the analyst; or photolysis may be used. There have been numerous papers that have been published recently that describe the use of HG-ICP-MS. , 1994).

1993). Other researchers have coupled different types of chromatography with HG-ICPMS to obtain speciation data. However, one of the major problems with this technique is obtaining full recovery of all the species present without altering the speciation. This obviously prohibits the use of conventional acid digestion of solid samples. Arsenic speciation has been achieved as reported in papers by Le et al. (1994) and Rubio et al. (1993). This latter paper is interesting because it involved on-line photooxidation to convert the nonreducible species into ones that can form hydrides.

P. Canadian Mineralogist 1995, 33, 303. I. Anal. Chim. Acta 1995, 312, 57. L. Spectrochim. Acta 1995, 50b, 803. J. Anal. At. Spectrom. 1995, 10, 89. , Ebdon, L. Spectrochim. Acta 1993, 48b, 1563. Gray, A. Anal. Proc. 1994, 31, 371. L. Spectrochim. Acta 1986, 41b, 151. L. Chem. Geol. 1995, 124, 91. J. Anal. At. Spectrom. 1994, 9, 605. E. Am. Lab. 1995, 27, 24. , Lichte, EE. Analyst 1995, 120, 2707. , Yoffe, D. J. Anal. At. Spectrom. 1993, 8, 475. J. Geochem. Explor. 1992, 44, 201. , Ohman, P. J.

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